Upgrade to Zebron from any 14 % cyanopropylphenyl / 86 % dimethylpolysiloxane phase:
| Agilent® | Restek® | SGE® | Supelco® | OV® |
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| DB®-1701 | Rtx®-1701 | BP10 | SPB®-1701 | OV-1701 |
| CP-Sil 19 CB | Rtx-VMS | Equity®-1701 |
Good Peak Shape for Active Analytes
Aromatic Amines by GC-MS
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Column:
Zebron ZB-1701
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Dimension:
30 meter x 0.25 mm x 0.25 µm
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Part No.:
7HG-G006-11
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Injection:
Split 15:1 @ 220 °C, 1 µL
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Oven Program:
60 °C for 1 min to 110 °C @ 30 °C/min to 135 °C @ 9 °C/min to 260 °C @ 30 °C/min for 2 min
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Detector:
MSD @ 180 °C
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Samples:
Analytes are at 1.58 mg/mL each
1. Piperidine
2. 2-Methylpiperidine
3. Aniline
4. Benzylamine
5. α-Phenylethylamine
6. N-Methylaniline
7. m-Toluidine
8. o-Toluidine
9. N,N-Dimethylaniline
10. β-Phenylethylamine
11. N-Ethylaniline
12. 2,4-Dimethylaniline
13. N,N-Diethylaniline
14. Dibenzylamine
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Orthogonal Selectivity for Separation
Oxygenated Compounds and Hydrocarbons in Alternative Fuels by Two Dimensional Gas Chromatography using Zebron ZB-1701 and ZB-1 GC Columns
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Column 1:
Zebron ZB-1701
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Phase:
14 % Cyanopropylphenyl 86 % Dimethylpolysiloxane
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Dimension:
30 meter x 0.25 mm x 0.25 μm
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Part No.:
7HG-G006-11
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Column 2:
Zebron ZB-1
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Phase:
100 % Dimethylpolysiloxane
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Dimension:
1.5 meter x 0.1 mm x 0.10 μm
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Part No.:
7TB-G031-02-C (2 meter trim to 1.5 meter)
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Sample:
Coal-derived Oil
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Injection:
Split 100:1 @ 250 °C, 0.5 μL
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Recommended Linear:
Zebron PLUS Straight Z-Liner™
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Part No.:
AG2-0A03-05
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Instrument:
Leco Pegasus 3, Agilent 6890N
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Carrier Gas:
Helium @ 1.5 mL/min (Constant Flow Mode)
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Oven Program:
50 °C for 0.3 min, to 300 °C at 2 °C/min
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Modulation:
Dual Jet Cryogenic, Liquid Nitrogen
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Modulation Period:
7 seconds
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Detection:
Flame Ionization (FID) @ 370 °C
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Hydrogen:
30 mL/min
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Air Flow:
400 mL/min
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